ONH836系列:氧氮?dú)浞治鰞x(熔融法)軟件特點(diǎn)和優(yōu)勢Cornerstone氧氮?dú)浞治鲕浖殖?個主要部分:分析、診斷、設(shè)定、儀器,界面可以快速導(dǎo)航和組織。工具條、滑動條和下拉式菜單簡化了校正和數(shù)據(jù)處理的參數(shù)設(shè)定。分析軟件同時包括實(shí)時的環(huán)境參數(shù)的監(jiān)測,提供完整的系統(tǒng)圖表模擬。高級診斷程序包括全數(shù)字化的在線操作手冊、維護(hù)模擬演示、圖片說明等提供快速指導(dǎo)。Cornerstone氧氮?dú)浞治鲕浖瑫r支持***的數(shù)據(jù)文檔格式和可變的報告格式。上海禹重實(shí)業(yè)有限公司致力于提供分析儀,有需要可以聯(lián)系我司哦!山東元素分析儀供應(yīng)商
SamplePreparationTypically,titaniumandzirconiumsamplesarechemicallyetchedtoremovesurfacecontaminationwhenoxygenandnitrogenaredetermined.However,etchingcanintroducehydrogenintothesample.ASTMmethodE1409"DeterminationofOxygenandNitrogeninTitaniumandTitaniumAlloysbytheInertGasFusionTechnique",asupdatedin1996,permitseitheretchingorabrading(filing)ofthetestspecimen.ASTME1447"DeterminationofHydrogeninTitaniumandTitaniumAlloysbytheInertGasFusionThermalConductivity/InfraredDetectionMethod"permitssurfacepreparationbyabrading(ifnecessarytoremovecontamination).DifferencesinsamplepreparationpresentsomewhatofadilemmaregardingsimultaneousdeterminationofO,N,andHintitanium.However,abradingsampleswithafiletoremovesurfacecontaminationwillyieldaccurateO,N,andHresults.TheONH836utilizesahigh-powerelectrodefurnacetoquicklyandefficientlyreleasethetargetgasesfromwithinthesample,whichallowsforaveryrapidsimultaneousdeterminationofoxygen,nitrogen,andhydrogen.廣東專業(yè)元素分析儀優(yōu)惠價格上海禹重實(shí)業(yè)有限公司為您提供分析儀,歡迎新老客戶來電!
Procedure–Powder/ChipSamplesInstrumentcalibration/driftcorrection.Addapproximately0.05gof***GraphitePowdertoa***GraphiteCrucible.Firmlyplacethecrucibleonthelowerelectrodetiporappropriateautoloaderposition.PresstheAnalyzebuttonontheinstrumentscreen,thelowerelectrodewillcloseandtheanalysissequencewillstartandendautomatically.Repeatsteps3bthrough3iaminimumofthreetimesforeachcalibration/driftstandardused.
氧氮?dú)浞治鰞x是快速、準(zhǔn)確分析氧、氮、氫元素的、高性能儀器,整機(jī)采用模塊化、一體化設(shè)計,即主機(jī)由可靠的脈沖電極爐、高靈敏高精度的檢測系統(tǒng)、布局合理和氣密性好的氣路系統(tǒng)、可靠耐用的電源系統(tǒng)、穩(wěn)定的電路系統(tǒng)、高校節(jié)能的水循環(huán)散熱系統(tǒng)等六個**的硬件模塊單元組成。氧氮?dú)浞治鰞x的測量原理:測量范圍非常***。分析樣品時,樣品被稱重后放到樣品端口中,然后用載氣進(jìn)行沖洗,防止大氣(含氧氣和氮?dú)猓┻M(jìn)入到爐子系統(tǒng)中。石墨坩堝在脈沖爐中脫氣,以盡量減少自帶的污染。經(jīng)過穩(wěn)定階段后樣品落入坩堝中并熔融。樣品中的氧與石墨坩堝中的碳反應(yīng)生成一氧化碳。氮和氫以單質(zhì)的形式釋放。載氣和樣品氣體通過粉塵過濾網(wǎng)后再進(jìn)入到氧化銅催化爐中,將一氧化碳氧化成二氧化碳。二氧化碳進(jìn)入到紅外池中用于測定氧含量,被測后的氣體導(dǎo)入化學(xué)試劑管,這時二氧化碳和水被化學(xué)試劑除去,氮元素通過熱導(dǎo)檢測池含量被測定。測量氫時,載氣換為氮?dú)?,樣品氣體通過舒茨試劑而不是氧化銅催化劑。測氧和氮時也可采用更廉價的氬氣作為載氣。上海禹重實(shí)業(yè)有限公司是一家專業(yè)提供分析儀的公司,歡迎您的來電哦!
Determinetheinstrumentblank.a.Loginaminimumof3Blankreplicates.b.PresstheAnalyzebuttonontheinstrumentscreen.Afterashortdelay,theloadingheadslide-blockwillopen.c.PresstheAnalyzebuttonontheinstrumentscreenagain,theloadingheadslide-blockwillcloseandthelowerelectrodewillopen.d.Cleantheupperandlowerelectrodemanually,or,ifapplicable,removethecrucibleandpresstheanalyzebuttontocleanwiththeautomaticcleaner.e.Firmlyplaceagraphitecrucibleonthelowerelectrodetip.f.PresstheAnalyzebuttonontheinstrumentscreen,thelowerelectrodewillcloseandtheanalysissequencewillstartandendautomatically.g.Repeatsteps2bthrough2faminimumofthreetimes.h.Settheblankfollowingtheprocedureoutlinedintheoperatorsinstructionmanual.上海禹重實(shí)業(yè)有限公司是一家專業(yè)提供分析儀的公司,有需求可以來電咨詢!廣東專業(yè)元素分析儀優(yōu)惠價格
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SamplePreparationSamplingandsamplepreparationisanimportantissuebecausetraditionalmethodsusedtoobtainsamplesforoxygenandnitrogendeterminationaredifferentfromthoserecommendedforhydrogen,especiallywhensamplingmoltenmetal.Themaindifferenceinsteelsamplingproceduresforoxygen/nitrogenandhydrogenisduetothemobilityofhydrogen.Specialprecautionsmustbeusedwhensamplingforhydrogen.Frommoltensteelandiron,asamplemustbequicklyquenchedincoldwaterandchilledinarefrigerantsuchasliquefiednitrogenoramixtureofacetoneandsolidcarbondioxideinordertoreducelossesofhydrogenfromdiffusion.Lossesofoxygenandnitrogenfromdiffusionarenotaproblem.Asamplethatistakenforhydrogenandchilledinarefrigerantcanalsobeusedforoxygenandnitrogendetermination.However,asamplethatistypicallytakenforoxygenand/ornitrogendeterminationisnotsuitableforhydrogendeterminationduetohydrogenloss(diffusion).Surfacecontaminationmustberemovedbyfilingorlightgrinding,usingcarenottooverheatthesample.山東元素分析儀供應(yīng)商